”Optimisation” of imaging conditions for weak beam studies of dislocation core structures in Ti3Al

نویسنده

  • J. Wiezorek
چکیده

The imaging conditions for weak beam (WB) studies of dislocations in Ti3AI with intermediate voltage transmission electron microscopes have been derived following a theoretical examination of the traditional criteria for WB-microscopy. The cores of <2c+a>-dislocations in room temperature deformed Ti3AI have been characterised in a case study with 300kV electrons by experimental WB-microscopy, which used imaging conditions not satisfying the traditional WB criteria. Image simulations facilitated the determination of the corrected dislocation dissociation widths for dissociated edge character dislocations. A superpartial separation of 19.5nm has been determined from experimentally observed image peak separations of (2lf 1)nm for the edge dislocation cores.

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تاریخ انتشار 2016